Diethyl (2-(4-Phenyl-1H-1,2,3-triazol-1-yl)benzyl) Phosphate
نویسندگان
چکیده
Here we describe a full structural elucidation of the diethyl (2-(4-phenyl-1H-1,2,3-triazol-1-yl)benzyl) phosphate. This compound is common by-product present in synthetic protocols to access α-hydroxy phosphonate compounds through Phospha-Brook rearrangement. Thus, complete NMR characterization this rearrangement was performed by 1H, 13C{1H}, 31P{1H}, COSY, HSQC, and HMBC experiments. Additionally, have demonstrated that 1H-31P 2D heteroatom experiment which combines simple identification 31P chemical shift with detection sensitivity 1H spectrum practical procedure.
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ژورنال
عنوان ژورنال: Molbank
سال: 2021
ISSN: ['1422-8599']
DOI: https://doi.org/10.3390/m1223